文档介绍:Instrumental Analysis
Shanghai University
Contents
Introduction
Introduction to Optical Methods
Atomic Emission Spectroscopy
Atomic Absorption Spectroscopy
The Absorption of Radiation: Ultraviolet and Visible
Molecular Luminescence:Fluorometry and phosphorimetry
The Absorption of Radiation: Infrared
Introduction to Electrochemical Methods
Potentiometry
Polarography
Introduction to Interphase Separations
Gas Chromatography
Liquid Chromatography
Chapter 1 Introduction
Definition of Instrumental Analysis
Classification
Function
Important Considerations
. The Definition of Instrumental Analysis
The science and art of determining position of materials with the instrumental methods based on a physical property characteristic of a particular element pound
Chemical Information observable Signal
by determination of physical properties
. Physical Properties Useful in Instrumental Analysis
1. Interaction of Radiant Energy with Matter
2. Electrical or Electrochemical Properties
3. Inter phase Separation
4. Other Properties
     Mechanical Properties
     Thermal Properties
     Nuclear Properties
      Extensive Properties
.Classification of Main Instrumental Methods
1. Optical Methods
Atomic: Absorption Spectroscopy,
Emission, Spectroscopy
Fluorescence Spectroscopy
Molecular: UV-Vis. Spectrophotometry
IR Spectroscopy
2. Electrochemical Methods
Potentiometry
Polarography
Voltammetry
3. Chromatography
Gas Chromatography
Liquid Chromatography
Basic Function of Instrumentation
Signal Generators
Input Transducers
Signal Transformation Modules
Output Transducers
Major Areas of an Instrumental Method
How the method “works”
Advantages and limitations of the method
Illustrative instrumentation
Applications
Problems
Bibliography
Chapter 2 Introduction to Optical Methods
The Nature of Radiant Energy
Spectral Regions
Interaction of Radiation with Atom and Molecule
Practical Sources of Radiation
Spectrograph and Monochr