文档介绍：anic Chem Lab
Survival Manual
A Student's Guide
to Techniques
James W. Zubrick
Hudson munity College
John Wiley & Sons
New York Chichester Brisbane Toronto Singapore
Copyright O 1984,1988,by John Wiley & Sons, Inc.
All rights resewed. Published simultaneously in Canada.
Reproduction or translation of any part of
this work beyond that permitted by Sections
107 and 108 of the 1976 United States Copyright
Act without the permission of the copyright
owner is unlawful. Requests for permission
or further information should be addressed to
the Permissions Department, John Wiley & Sons.
Library of Congress Cataloging-in-Publication Data
Zubrick, James W.
anic chem lab survival manual.
Includes indexes.
1. Chemistry, Organic -Laboratory manuals.
I. Title.
1988 547'.0078 87-20968
ISBN 0-471-85519-7(pbk.)
Printed in the United States of America
To Cindy
Preface to the
Second Ed it ion
It is heartening to hear of your book being read and enjoyed, literally cover to
cover, by individuals ranging from talented high-school science students to
Professors Emeritus of the English language. Even better to hear that you
have a chance to improve that book, based upon the ments,
comments by reviewers, and the experience gained from working with the
text.
In this edition of anic Chem Lab Survival Manual, the section on
notebooks and handbooks have been expanded to include typical notebook
pages and actual handbook entries along with interpretation. There are new
notes on cleaning and drying glassware, and how to find a good recrystalliza-
tion solvent. Once their samples are purified, students may now find direc-
tions for taking a melting point with the Thomas-Hoover apparatus. Wash-
ing has been given the same importance as extraction, and a few more trouble
spots -taking the pH of anic layer, for one - have been smoothed.
There are additional instructions on steam distillation using