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硕博学位论文
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臝DELOPNTProfdrirWeidongMaterials,InstituteMayofthefor琘CYCLOHEXANONE匣SubmittedtheScienceLeiJiangKeyCatalysisTS1FORZhua
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TS1摘要TS1间体。随着己内酰***需求量的逐年增加，环己***肟的需求量也在持续增长。传统法合成环己***肟是经过环己***一羟***路线，由于在生产过程中使用了有毒的羟***TSl低的技术瓶颈，且使用昂贵模板剂四丙基氢氧化铵贾耇合成成TS1TPAOH昧勰０寮琳“，瓸替代部分铣闪薚。降低了合nlnTs16EniChemSpATS1本较高。TS1XRDSEM、癗迅降缺碚魇侄味院铣傻腡进行分析，同时考察其在环己***氨氧化反应中的催化性能。本论文的主要研究结果如下：成成本。TS1500应中有很好的催化性能。TS1能。2
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ⅪDEVELOPNTsamples胛一0XIFORATl0NCYCLOHEXANONEsynthesis琣synthesizedTS1Aofcaprolactam(CPL)asynthesisWithcyclohexanone-hydroxylamine瑆hydroxide(TPAOH)fortheand琒，，琣甌琾hydroxylamineenvironmentalLater,theextra-frameworktetrapropylammoniumsynthesismethodsincharacterizedvarious—．瑃ammoximmionareThecyclohexanoneoximekeyformanufactureNylon-6瑃瓵traditional—routeinwhichtoxiccorrosive琹ItaliancompanyEniChemSpAdevelopedeffectiveprocessHowever,in瑃Tispeciesavailablelowquadridentate-frameworksamplesAdditionally,theexpensiveleadingdevelopcheapwasusedinsteadexpensiveTPAOHtoframeworkuniformcrystalsynthesizedThencatalyticcatalystsevaluated甌resultsfollowscheaperinstead瑆costscurrentaⅡ
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frameworkKEYWORDSTS1cyclohexanonecyclohexanonesamplesuniformsmallerthesynthesissimpleroximeammoxidation一琹lowerresultantTS1甌Tispeciesandcrystalsizes500synthesizedviaprocessconditionsTheTS1catalystsexcellentcatalyticcyclohexanoneThenovelty：·，whichshorterInadditionthecyclohexanonecompared．costsnlnIII
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