文档介绍:广藿香叶药材质量标准研究
宋丽莉(广州王老吉药业股份有限公司广东广州 510450)
【中图分类号】R282 【文献标识码】B【文章编号】1672-5085(2013)25-0412-02
【摘要】目的研究制定广藿香叶药材的质量标准。方法采用百秋李醇作为对照品,对广藿香叶进行薄层色谱鉴别,同时采用气相色谱法进行含量测定,HP-5毛细管柱;检测器FID,柱温采用程序升温。结果薄层鉴定:特征性强;含量测定方法,操作简单,准确,~,回归方程为Y=-,R2=(n=7),%,RSD=%(n=6)。结论所采用的定性、定量方法准确、简便,灵敏、结果可靠,为研究评价广藿香叶药材质量提供了一定的依据。
【关键词】广藿香叶百秋李醇薄层色谱鉴别气相色谱法
Studies on the Quality Standard of Pogostemonis Folium
Song Lili(Guangzhou Wanglaoji pany Limited ,Guangdong Guangzhou 510450)
【Abstract】:Objective: To establish a quality standard for Pogostemonis Folium. Method: We use Patchouli Alcohol as a reference substance to identify Pogostemonis Folium by TLC and to determine the content by GC. We use HP - 5 capillary column, FID detector and temperature programmed. Results: The method of TLC is Characteristic and method of content determination is simple and accurate. Patchouli Alcohol shows a good linear relationship within the range of ~ . The regression equation for Y = x - , R2 = (n = 7) and the average recovery is %,RSD=%(n=6).Conclusion: Methods we used are simple and accurate and showed reliable results. These methods can be used for the study of quality standard of Pogostemonis Folium。
【Key words】 Pogostemonis Folium Patchouli Alcohol TLC identification GC
本品为唇形科植物广藿香Pogostemon cablin (Blanco) Benth.