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浸渍法制备整体式TS-1催化剂.pdf

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浸渍法制备整体式TS-1催化剂.pdf

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文档介绍:Preparation of TS-1 Monolithic Catalysts by Dip-coa ting Wenhao Yu a, Libin Yang *a,b, Feng Xin b, Jianjun Yuan a a Tianjin Key Laboratory of Marin Resources and Chemi stry, Tianjin University of Science and Technology, Tianjin 300457, China; bSchool of Chemical Engineering and Technology, Tian jin University, Tianjin 300072, China; ******@tust. Keywords: TS-1 deposited film, monolithic catalysts, dip-coa ting, pretreatment, cordierite b ceramics, washing out, immobilized Abstract. TS-1 monolithic catalysts were prepared on cordier ites b ceramics supports by dip-coating method in TS-1/H 2O suspension. The cordierites b ceramics su pports were treated with different methods, such as coated with a thin layer of sodium silicate, immersed in hydrochloric acid. The monolithic catalysts were ch aracterized by Scanning Electron Microscopy. The distribution of TS-1 Catalysts onto supported w as observed. The immobilized stability of TS-1 monolithic catalysts was evaluated by ultrasonic cl eaning and washing out experiment. TS-1 catalysts were uniformly deposited onto inner smoothed surfac e of cordierites b ceramics supports, which ware coated sodium silicate film. And experim ent data proved that TS-1 catalysts may be firmly immobilized onto supports coated sodium sili cate. Introduction Titanium silicate-1 (TS-1