文档介绍:Notes J . Org. Chem., Vol. 62, No. 21, 1997 7513
Ta ble 1. 1H NMR Da ta
proton mult CDCl3 (CD3)2CO (CD3)2SO C6D6 CD3OD D2O
solvent residual peak
H2O s
acetic acid CH3 s
acetone CH3 s
acetonitrile CH3 s
benzene CH s
tert-butyl alcohol CH3 s
OHc s
tert-butyl methyl H3 s
OCH3 s
BHTb ArH s
OHc s
ArCH3 s ArC(CH3)3 s
chloroform CH s
cyclohexane CH2 s
1,2-dichloroethane CH2 s
dichloromethane CH2 s
diethyl ether CH3 t, 7
CH2 q, 7
diglyme CH2 m
CH2 m
OCH3 s 1,2-dimethoxyethane CH3 s
CH2 s
dimethylacetamide CH3CO s
NCH3 s