文档介绍：硅酸盐学报
第 34 卷第 5 期 Vol. 34 No. 5
2006 年 5 月 JOURNAL OF THE CHINESE CERAMIC SOCIETY May 2006

沉淀法制备钨酸铅纳米粉体

王卓 1 杨玉国 2 杨长红 2
1. 烟台大学环境和材料工程学院山东烟台 264005 2. 山东大学晶体材料国家重点实验室济南 250100

摘要以钨酸钠和硝酸铅为原料以聚乙二醇 200 为分散剂用沉淀法配制出钨酸铅混浊液将钨酸铅混浊液在 100 烘干后制备出钨酸铅纳米
粉体对制备的样品进行 X 射线衍射分析结果表明钨酸铅纳米粉体结晶良好将制备的样品在不同温度退火后用透射电镜分析了其形貌结
果表明钨酸铅纳米粉体的颗粒粒度随着退火温度的升高而增大

关键词钨酸铅沉淀法纳米粉体
中图分类号文献标识码 A 文章编号 0454–5648(2006)05–0601–03

PREPARATION OF LEAD TUNGSTATE NANO-PARTICLES BY DEPOSITION METHOD

WANG Zhuo1 YANG Yuguo2 YANG Changhong2
(1. School of Environment and Materials Engineering, Yantai University, Yantai 264005, Shandong; 2. State Key Laboratory of
Crystal Materials, Shandong University, Jinan 250100, China)

Abstract: Lead tungstate nano-particles were prepared by deposition after being heat-treated at 100 , using lead nitrate and natrium
tungstate as starting materials and polyglycol 200 as dispersant. The XRD pattern indicates that the well crystalized lead tungstate
nano-particles were obtained under the given synthesis conditions. The prepared nano-particles were heat-treated at different
temperatures. Transmission electron microscopy was used to study their morphologies. The results show that the sizes of
nano-particles increase with the increaseing of annealing temperatures.

Key words: lead tungstate; deposition; nano-partic