文档介绍：2008年第28卷第1期,151~,151~154研究简报·超声辐射下合成1_[(未)取代苯酰基一3一[5一(1一苯基一3一甲基-5-氯吡唑一4一基)一1,3,4一噻二唑一2一基】一硫脲孙燕荣李燕萍刘晨江,6王吉德6新疆大学化学化工学院石油天然气精细化工教育部重点实验室乌鲁木齐830046)(西安交通大学理学院西安710049)(1一苯基一3一甲基一5一氯吡唑-4一基)一1,3,4一噻二唑(1),然后分别采用超声辐射法和常规加热法与(未)取代苯甲酰基异硫氰酸酯(2)反应合成了一系列未见报到的1一【(未)取代苯酰基一3一【5()一1,3,(3a~3j).化合物的结构经元素分析,IR,;(未)取代苯甲酰基硫脲;1,3,4-_噻二唑;吡唑;合成Synthesisof1-[(Un)substitutedbenzoy1]-3_[5一(1一phenyl一3一methyl一5一chIoropyrazoIe一4一yI)一1,3,4-,thiadiazol一2一yq‘thioureaunderUItrasonicRadiationSUN,Yan—Rong'LI,Yan.-Ping'LIU,Chen..Jiang,“,WANG,Ji—De“,(“KeyLaboratoryofPetroleumandGasFineChemicals,MinistryofEducation,CollegeofChemistryandChemicalEngineering,XinjiangUniversity,Ulumqi830046)(SchoolofSciences,XianJiaotongUniversity,Xian710049)Abstract2-Amino--5一(1·-phenyl一3一methyl-5一chloropyrazol一4一y1)一1,3,4一thiodiazole(1)hasbeenpreparedbythereactionof1-phenyl--3一methyl一5一chloropyrazol一4一,[(un)substitutedbenzoy1]一3一[5一(1·-phenyl一3一methyl-5一chloropyrazole-_4一y1)一1,3,4一thiadiazol一2-y1]一thioureas(3a~3j)pound1with(un)substitutedbenzoylisothiocyanates(2),;(fun)substitutedbenzoylthiourea;1,