文档介绍：Organic Experiments
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Experiments
Seventh Edition
Louis F. Fieser
Late Professor Emeritus
Harvard University
h L Williamson
Mount Holyoke College
D. C. HEATH PANY
Lexington, Massachusetts Toronto
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D. C. Heath
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Cover: Charlotte Raymond/Science Source/Photo Researchers, Inc.
Copyright © 1992 by D. C. Heath pany.
Previous editions copyright © 1987, 1983, 1979, 1975, 1968, and 1964 by D. C.
Heath pany.
All rights reserved. No part of this publication may be reproduced or
transmitted in any form or by any means, electronic or mechanical, including
photocopy, recording, or any information storage or retrieval system, without
permission in writing from the publisher.
Published simultaneously in Canada.
Printed in the United States of America.
International Standard Book Number: 0-669-24344-2
Library of Congress Catalog Number: 91-71287
10 9 8 7 6 5 4
Preface
Organic Experiments, Seventh Edition, presents to the beginning student a
series of clear and concise experiments that encourage accurate observa-
tion and the development of deductive reasoning.
New to this edition is the section at the end of every experiment
entitled "Cleaning Up," which has been written with the intent of focusing
students' attention not just on the desired product from a reaction, but also
on all of the other substances produced in a anic reaction.
Throughout the text most, but not all, of the 60 and 90 MHz nmr spectra
have been replaced with 250 MHz proton spectra. A section on 2D nmr is
included in the chapter on nmr spectroscopy, and procedures are given for
the use of chiral nmr shift reagents to determine the optical purity of the
product from the chiral enzymatic reduction of a ketone.
A number of small changes have been made so anic Experi-
ments reflects the very latest and best anic chemistry. Nomenclature
revision is a continuous process. Gradually names su