文档介绍：11 1
现代食品科技 Modern Food Science and Technology 2011, ,

高效液相色谱法检测甘蔗中莠去津的残留量

缪璐,莫佳琳,胡振洲,干宁军
(国家食糖及加工食品质量监督检验中心,广西南宁 530022)
摘要:本论文建立了高效液相色谱快速测定甘蔗中莠去津的方法。甘蔗经加速溶剂萃取仪萃取,应用高效液相色谱仪定量法检测
莠去津,建立了定量检测甘蔗中莠去津快速、准确、高灵敏度的方法。经方法学验证,该方法对莠去津最低检出限 LOD 为 mg/kg。
在 ~ μg/mL 的线性范围中,相关系数 r>,平均回收率:%~%。结论:方法灵敏度高、操作简单、定量准确、测定
浓度范围广,是甘蔗样品中莠去津含量检测的理想方法。
关键词:高效液相色谱,莠去津,加速溶剂萃取
文章篇号:1673-9078(2011)6-713-714
Determination of Atrazine in Sugar Cane by HPLC
MIAO Lu, MO Jia-lin, HU Zhen-zhou, GAN Ning-jun
(National Supervision & Testing Center for Quality of Sugar and Processed Food, Nanning 530022, China)
Abstract: High performance liquid chromatography (HPLC) method was developed for the determination of atrazine in sugar cane extracts
by ASE. This method was fast, accurate and highly sensitive. The limit of detection (LOD) for atrazine was . The linear range was
- μg/mL with correlation coefficient above . The mean recovery was between % and %。This method can be applied for
the determination of atrazine in sugar cane for its high sensitivity and high selectivity.
Key words: HPLC; atrazine; ASE

莠去津(atrazine)又名阿特拉津,是一种化学除草剂器厂。
[1],主要用于防除玉米、高梁和甘蔗等作物田中各种阔莠去津标准物质,购自国家标物中心;甲醇(色谱
叶杂草及禾本科杂草。我国从 60 年代开始引进莠去津, 纯),美国 Fishier Scientific 公司;实验用水为超纯水。
近年来,莠去津被广泛应用在各甘蔗产区,使用量也成实验条件
倍增长。莠去津较长的残留期(一年